| 水热合成反应釜也称为溶样器、压力溶弹、水⊙热合成釜、高温高压消解罐、聚四氟乙烯高压罐是为在一定温度、一定压力条件下合成化学物质提供的反应器。它广泛应用于新材料、能源、环境工程等领域的科研试验中，是高校教学、科研单位进行科学研究的常用小型反应器。 2．特点 本水热合成反应釜采用优质不锈钢加工而成。釜体与釜盖密封采用耐用、可靠的线〓密封结构，密封效果长期稳定无泄漏。 本水热合成反应釜采用外加热方式，以缩小体积，并有利多反应釜处于同一反应操作温度（如将ζ多个反应釜置于烘箱中加热）。 3．主要技术指标 （1）．工作温度：≤230℃ （2）．工作压力：≤3MPa（表压） （3）．升温、降温速率：≤5℃/min （4）. 规格25，50，100，120，200ml另∞可根据用户需求定做。 4.操作方法 将反应物系指与釜体内，并保证加〇料系数小于0.8。当反应物系有腐蚀性时要』将其置于四氟衬↙套内，方可保证▃釜体不受腐蚀。将水热合成反应釜置于加热器内，按照规定的升温速率升温至所需╱反应温度（小于规定的安全使用温度）。待反应结束将其降温时，也要严格按照规定的降温速率操作，以利安全和反应釜的使用★寿命。当确认腹内温度低于『反应物系种溶剂沸点后方能打开釜盖进行后续操作。
每次水热合︽成反应釜使用后要及时将其清☉洗干净，以免锈蚀。
釜体、釜盖线密封处要格外注意清洗干净，并严防将其碰伤损坏。
Hydrothermal synthesis reactor, also known as digestion, pressure melting bombs, hydrothermal synthesis reactor, high temperature and pressure digestion vessels, PTFE high-pressure tank is in a certain temperature and pressure conditions, certain synthetic chemicals supplied reactor. It is widely used new materials, energy, environmental engineering and other fields of scientific research and experiments, is university teaching, scientific research units commonly used small reactors.
2. Feature
The hydrothermal synthesis reactor using high-quality stainless steel processing. Kettle kettle lid body and sealed with durable, reliable cable seal structure, the sealing effect long-term stability without leakage.
The hydrothermal synthesis reactor with external heating, to reduce the volume and more favorable reaction in the same reactor operating temperature (such as multiple reactor placed in an oven heated).
3. Main indicators
(1). Operating temperature: ≤ 230 ℃
(2). Working pressure: ≤ 3MPa (gauge)
(3). Heating, cooling rate: ≤ 5 ℃ / min
(4) specification 25,50,100,120,200 ml other customized according to user needs.
4 methods of operation
The reaction means and the reactor body, and to ensure feeding coefficient is less than 0.8. When the Department of corrosive reaction when you want to put PTFE bush, can only be assured kettle body from corrosion. Hydrothermal synthesis reactor will be placed on the heater, in accordance with the provisions of the heating rate of heating to the desired reaction temperature (less than the required safety temperature). Completion of the reaction will be when its cool, but also in strict accordance with the provisions of the cooling rate operation, to facilitate the safety and reactor life. When confirmation of intra-abdominal temperature below the boiling point solvents reaction system can only open the tank lid after a follow-up operation.
Hydrothermal synthesis reactor each time after use to clean, to avoid corrosion.
Kettle body, kettle lid seal line to pay particular attention to clean and prevent damage to the bumps |
