HIRALPAK® IC：硅胶表面共价键合有纤维素-三（3,5-二氯苯基氨基甲酸酯）；耐溶剂型手性柱，溶剂使用无限制，可使用任何互溶的溶剂作为流动相、溶解样品，手性柱再生。CHIRALPAK® IC具有广泛的拆分能力，在分析中得到广泛的应用，主要分离酰胺基、芳香环取代基、羰基硝基、磺酰基、氰基、羟基、氨基衍生物等。CHIRALPAK® IC短柱不但具有广泛的分析能力，而且具有柱效高、分析快速的特点，可以节约大量的分析时间，可以分离：5,5-二苯基-4-甲基-2-噁唑烷酮、2-[(4-氯-邻用苯基)氧]丙酸、米氮平、N-FMOC-DL-Leucine、N-FMOC-DL-Phenylalanine、诺米芬辛、替马西泮、匹多莫德、兰索拉唑、利伐沙班等。
键合型手性柱的修复方式：
CHIRALPAK IA/IB/IC/ID
Step 1用EtOH0.5ml/min冲洗30min，再用100%THF0.5ml/min冲洗2h
Step2 用EtOH0.5ml/min冲洗30min过渡
Step3用正己烷/乙醇=80/20（v/v）冲洗色谱柱
Step4若效「果不好，将THF更换成100%DMF或DMAC0.3ml/min冲洗3h
CHIRALPAK IA-3/IB-3/IC-3/ID-3
Step1用EtOH0.5ml/min冲洗30min，再用100%THF0.5ml/min冲洗2h
Step2 用EtOH0.05ml/min冲洗300min过渡（低流速冲洗对提高手性柱理论塔板数很重要！）
Step3若效果不好，将THF更换成100%DMF或DMAC0.3ml/min冲洗3h
即日起购买TOSOH色谱柱及其保护柱、waters色谱柱、Silgreen色谱柱可以获得绿百草小耗材礼品一份，详情请☆咨询绿百草！
|
Compound |
5,5-Diphenyl-4-methyl-2-oxazolidinone/5,5-二苯基-4-甲基-2-噁唑烷酮 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
2.80 |
|
Compound |
7,8,9,10-Tetrahydrobenzo[a]pyren-7-ol |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
3.33 |
|
Compound |
Mecoprop/ 2-[(4-氯-邻用苯基)氧]丙酸 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
1.82 |
|
Compound |
Mirtazapine/米氮平 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
2.81 |
|
Compound |
N-FMOC-DL-Leucine |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
2.45 |
|
Compound |
N-FMOC-DL-Phenylalanine |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
2.68 |
|
Compound |
Nomifensine/诺米芬辛 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
4.19 |
Nomifensine
|
Compound |
Temazepam/替马西泮 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
5.38 |
Temazepam
|
Compound |
利伐沙班 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
3.60 |
|
Compound |
兰索拉唑 |
|
Column |
CHIRALPAK IC |
|
Column size |
4.6I.D.X150mm X 5um |
|
Resolution |
3.70 |
